Figure 13-6 Schematic representation \"of the effect of stress on creep curves at constant temperature. Figure 13-6 shows the effect of applied stress on the creep curve at constant temperature. It is apparent that a creep curve with three well-defined stages will be found for only certain combinations of stress and temperature. A similar family of curves is obtained for creep at constant stress for different temperatures. The higher the temperature, the greater the creep rate. 13-4 THE STRESS-RUPTURE TEST The stress-rupture test is basically similar to the creep test except that the test is always carried out to the failure of the material Higher loads are used with the stress-rupture test than in a creep test, and therefore the creep rates are higher. Ordinarily the creep test is carried out at relatively low stresses so as to avoid tertiary creep. Emphasis in the creep test is on precision determination of strain, particularly as to the determination of the minimum creep rate. Creep tests are frequently conducted for periods of 2,000 h and often to 10,000 h. In the creep test the total strain is often less than 0.5 percent, while in the stress-rupture test the total strain may be around 50 percent. Thus, simpler strain-measuring devices, such as dial gages, can be used. Stress-rupture equipment is simpler to build, maintain, and operate than creep-testing equipment, and therefore it lends itself more readily to multiple testing units. The higher stresses and creep rates of the stress-rupture test cause structural changes to occur in metals at shorter times than would be observed ordinarily in the creep test, and therefore stress-rupture tests can usually be terminated in 1,000 h. The basic information obtained from the stress-rupture test is the time to cause failure at a given nominal stress for a constant temperature. 97
The elongation and reduction of area at fracture are also determined. If the test is of suitable duration, it is customary to make elongation measurements as a function of time and from this to determine the minimum creep rate. The stress is plotted against the rupture time on a log-log scale (Fig. 13-7). A straight line will usually be obtained for each test temperature. Changes in the slope of the stress-rupture line are due to structural changes occurring in the material, e.g., changes from transgranular to intergranular fracture, oxidation, recrystallization and grain growth, or other structural changes such as spheroidization, graphitization, or sigma-phase formation. It is important to know about the existence of such instabilities, since serious errors in extrapolation of the data to longer times can result if they are not detected. Figure 13-7 Method of plotting stress-rupture data (schematic) 13-7 DEFORMATION MECHANISM MAPS A practical way of illustrating and utilizing the constitutive equations for the various creep deformation mechanisms is with deformation mechanism maps. Ashby and co-workers have developed these maps in stress-temperature space. The various regions of the map (Fig. 13-11) indicate the dominant deformation mechanism for that stress-temperature combination. The boundaries of these regions are obtained by equating the appropriate equations in Sec. 13-6 and solving for stress as a function of temperature. The boundaries represent combinations of stress and temperature where the respective strain rates for the two deformation mechanisms are equal. 98
We see for example, for the metal shown in Fig. 13-11 that at a homologous temperature of 0.8 and a low stress the deformation occurs by diffusional low (Nabarro-Herring creep). Keeping the temperature constant and increasing the stress we enter a region of power-law creep (dislocation creep) and at still higher stress the metal deforms by thermally activated dislocation glide. The upper bound on the diagram is the stress to produce slip in a perfect (dislocation free) lattice. Figure 13-11 Simplified deformation mechanism map. (After Ashby.) Contours of isostrain rate can be calculated from the constitutive equations and plotted on the deformation mechanism map (Fig. 13-12). Thus, in addition to identifying the dominant deformation mechanism the map allows selection of any two of the three variables, a, £, or T, and establishment of the third value. A deformation mechanism map is not only a useful pedagogical tool but it can be helpful in decisions involving alloy design and selection. 99
Figure 13-12 Deformation mechanism map for pure nickel with grain size of 32 µm. (M. F. Ashby, Acta Met., vol. 20, p. 3, 1972.) 13-9 SUPERPLASTICITY Superplasticity is the ability of a material to withstand very large deformations in tension without necking. Elongations in excess of 1,000 percent are observed. In Sec. 8-6 we showed that superplasticity was related to the existence of a high strain-rate sensitivity. In this section we deal more broadly with superplastic behavior and relate it to the appropriate high-temperature deformation mechanisms. Superplastic behavior occurs at T > 0.5Tm. Not only does the material show large extensibility without fracture but at low strain rates the flow stress is very low. Thus, complex shapes may be readily formed under superplastic conditions. The requirements for a material to exhibit superplasticity are a fine grain size (less than 10 µm) and the presence of a second phase which inhibits grain growth at the elevated temperature. 100
Most superplastic alloys are eutectic or eutectoid compositions. The strength of the second phase should be similar to that of the matrix phase to avoid extensive internal cavity formation. 101
NON-DESTRUCTIVE TESTING (NDT) Why use NDT? Components are not destroyed Can test for internal flaws Useful for valuable components Can test components that are in use 1. Penetrant testing Used for surface flaws. The oil and chalk test is a traditional version of this type of testing. Colored dyes are now used. 2. Magnetic particle testing Used for ferrous metals. Detects flaws close to the surface of the material. The component to be tested must first be magnetized. 102
Magnetic particles which can be dry or in solution are sprinkled onto the test piece. The particles stick to the magnetic field and flaws can be inspected visually by examining the pattern to see if it has been distorted. The component must be demagnetized after testing. 3. Eddy current testing Used for non-ferrous metals A.C. current is passed through the coil. The test piece is passed under the coil causing secondary currents called eddy currents to flow through the test piece. This causes a magnetic field to flow in the test piece. The flaws are detected on an oscilloscope by measuring a change in the magnetic field. 103
4. Ultrasonic testing Ultrasonic Sound waves are bounced off the component and back to a receiver. If there is a change in the time taken for the wave to return this will show a flaw. This is similar to the operation of a sonar on a ship. Operation. The ultrasonic probe sends the sound wave through the piece. The sound waves bounces off the piece and returns. The results are then placed on the display screen in the form of peaks. Where the peaks fluctuate this will show a fault in the piece. 104
Uses. This is generally used to find internal flaws in large forgings, castings and in weld inspections. 5. Radiography (X-ray) Testing The x-ray are released by heating the cathode. They are then accelerated by the D.C. current and directed onto the piece by the tungsten anode. The x-rays then pass through the test piece onto an x-ray film which displays the results. The x-rays cannot pass through the faults as easily making them visible on the x-ray film. Uses. 105
This is a test generally used to find internal flaws in materials. It is used to check the quality of welds, for example, to find voids or cracks. 106
CHAP NON DEST TEST
PTER 6 TRUCTIVE TING 1
❖ Many of the parts that ar like aircraft, ship or the inspected to make sure t that may lead to problems ❖ Even very small defects th magnification can somet must be found. NDT in equipment that can find they are buried inside the
re used in complex systems e Space Shuttle must be they do not contain defects s or accidents. hat can not be seen without times cause problems and nspectors use specialized these small defects even if material. 2
What i O Non – destructive test O used to inspect shipbu prove that their struct defects or faults such and porosity. O Testing procedures ha reveal both internal an without harming the m properties, appearanc usefulness.
is ndt? ts uilding components to ture is free from h as cracks, inclusions ave been designed to nd external faults material nor its ce, characteristics or 3
Applicatio O Casting defects O Welding or brazing defe O Crack detection (interna O Damage (delamination) O Material heterogeneity O Adhesion defects: O absence of adhesive O defect in adhesive O craks in adhesive O Electronics: defects in c
ons of NDT ects al or emergent) ) in composite materials e components attachment. 4
Vi Insp Eddy Current Testing Radiographic Testing Ultr Te
isual pection Liquid Dye Penetrant Testing Magnetic Particle Testing rasonic 5 esting
Visual Inspec O Visual inspection (VT) detection of surface im eye. O Normally applied with additional equipment, by using aids such as improve its effectivene
ctions Testing ) relies upon the mperfections using the hout the use of any , VT can be improved a magnifying glass to ess and scope. 6
Visual Insp Robotic c in hazard air ducts
pections Testing Most basic and common inspection method. The primary and oldest method of NDT Tools include fiberscopes, borescopes, magnifying glasses and mirrors. crawlers permit observation 7 dous or tight areas, such as s, reactors, pipelines.
Visual Inspec Advantages O Primary method of inspection O On-going inspection O Most economical inspection method O Applicable at any stage of fabrication. O relative simplicity O does not require sophisticated apparatus,
ctions Testing limitations O Restricted to surface inspection O Good eyesight required O Good lighting required O Person performing the inspection must know and be able to recognize what he/she is looking for. 8
Liquid Dye P ❑ Use to locate cracks, poros surface of a material. ❑ To inspect large areas ver nonporous materials.
Penetrant Testing sity and other defect that break the ry efficiently and will work on most 9
Liquid Dye Test O Liquid penetrant inspection (PT) re out” of a penetrating medium agai O This is done by applying penetrant of the item being inspected. O The penetrant is applied to the sur surface for a prescribed time (dwe O the penetrant liquid will be drawn i action. O Following removal of excess penetr reverses the capillary action and d O The resultant indications reveal the be visually inspected and evaluate
e Penetrant ting eveals surface flaws by the “bleed- inst a contrasting background. to the pre-cleaned surface and flaw rface and allowed to remain on the ell time); into any surface opening by capillary rant an application of a developer draws penetrant from the flaw. e presence of the flaw so that it can ed. 10
Method to STEP 1 STEP 2 PRE-CLEAN PENETRANT APPLICATION • Clean and dry the surface to be • Spray the surfac inspected. tested with coloured penetra usually red in colo STEP 6 STEP 5 INSPECT/ DEVELOPER EVALUATE APPLICATION • Inspect for defect. •Apply white develo inspection area a sufficient time for it
o Perform LPT ce to be STEP 3 visibly TIME FOR ating dye CAPILLARY ACTION our. • Allow sufficient time for capillary action to work and the dye to be absorbed into cavities R STEP 4 N EXCESS oper to the PENETRANT REMOVAL and allow t to work. • Remove excessive penetrant dye and wipe the surface clean a11nd dry
ABC DE
Penetrant testing: A : Sample before testing; B: Liquid penetrant applied; C: Surplus wiped off leaving penetrant in crack; D: Developer powder applied, dye soaks into powder; E: View coloured indications, or UV lamp shows up fluorescent indications. 12
Consumab Dye Penetrant D
ble used in LPT 13 Developer Cleaner
Example – B
Bicycle crank arm 14
Examp Crack Crack at attachment holes in hinge
ple of cracks ks in a weld Visual and magnetic test of crack 15 originating at hole
Liquid Dye P Advantages Simple and easy to conduct. Will detect surface and near surface flaws. Can detect flaws filled with contaminants e.g. oxide or non metallic inclusions. Components of any size and shape can be checked. Instrument are portable and easy to handle.
Penetrant Testing Limitations Will not detect deep internal flaws. Coatings and paintings will affect the testing methods. Detects only surface breaking defects. Surface preparation is critical as contaminants can mask defects. Requires a relatively smooth and16 nonporous surface
Magnetic P ❖ Used to locate surface and sl defects in ferromagnetic mate some of their alloys Yo
Particle Testing light subsurface discontinuities or erials such iron, nickel, cobalt, or oke 17
Magnetic P
Particle Testing 18
Method to P • Ensure the parts are clean, dry and fr Step 1 • Magnetize parts by applying magnetic Step 2 • Ensure that a strong circular magneti Step 3 the two prods. • Inspect test piece. The iron particles Step 4 identifying the position of any defects • Under testing inspection visually obse Step 5 around any defects, cracks or flaws c • Demagnetize the component under t Step 6
Perform MT ree from oil and grease. c particles ic field is passed through the test piece using adhere to the surface imperfections thus s, flaws and discontinuities erve if fine magnetic particles are gathered caused by flux magnetic leakage test 19
Magnetic Pa Indica
article Crack ations 20
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