Vapemate e-Liquid Samples May 2015

Vapemate 531 Park Lane Kenora, ON P9N 1A3, Canada e-Liquid Samples ECTA of Canada Analysis Report (0515-561) GC/FID Analysis (ENT184) Nicotine Diethylene glycol (DEG) HPLC/UV Analysis (ENT301) Acetaldehyde Acetoin (aka 3-Hydroxy-2-butanone) Diacetyl Formaldehyde 2,3-Pentanedione (aka Acetyl propionyl)General Lab Services (ENT058 & 072) pH Level Karl Fisher Titration, % Water Enthalpy Analytical, Inc. Phone: (919) 850 - 4392 / Fax: (919) 850 - 9012 / www.enthalpy.com 800-1 Capitola Drive Durham, NC 27713-4385

I certify that to the best of my knowledge all analytical data presented in this report:  Have been checked for completeness  Are accurate, error-free, and legible  Have been conducted in accordance with approved protocol, and that all deviations and analytical problems are summarized in the appropriate narrative(s)This analytical report was prepared in Portable Document Format (.PDF) and contains 13 pages. Report Issued: 7/2/2015 EA# 0515-561 Page 2 of 13

Summary of Results EA# 0515-561 Page 3 of 13

Testing Cert. # 3198.01Report for: Vapemate Project Code: 0515-561Client Project: ECTA of Canada Project Start Date: 5/26/15Sample Type: e-Liquid Analysis Method: ENT184Enthalpy Code Client Sample ID Notes Nicotine0515-561-01-1 ECTA0004-017A (mg/mL)0515-561-01-2 ECTA0004-017A Melon Dram 6mg Melon Dram 6mg 4.67 4.67 Average 4.67 % DIFF 0.10515-561-02-1 ECTA0004-018A VM Tobacco 0mg < 0.500 ND0515-561-02-2 ECTA0004-018A VM Tobacco 0mg < 0.500 ND < 0.500 ND Average % DIFF NA0515-561-03-1 ECTA0004-019A Papa Mgo 24mg 21.10515-561-03-2 ECTA0004-019A Papa Mgo 24mg 21.5 21.3 Average 1.9 % DIFFND: Not Detected; analyte not detected above the MDL0515-561 v0.1 nic, Nico (2)Page 1 of 1 7/1/20153:58 PM EA# 0515-561 Page 4 of 13

Report for: VapeMate Project Code: 0515-561Client Project: ECTA of Canada Project Start Date: 5/26/15Sample Type: e-Liquid Analysis Methods: ENT184Enthalpy Code Client Code Notes Diethylene glycol 0515-561-01 ECTA0004-017A (ug/mL) 0515-561-02 ECTA0004-018A 0515-561-03 ECTA0004-019A < 4.45 ND < 4.45 ND < 4.45 NDND: Non Detect or analytical result below the MDL and is less than (<) the reported value.0515-561 DEG v0.5, DEG 7/2/2015Page 1 of 1 7:19 AM EA# 0515-561 Page 5 of 13

Report for: VapeMate Project Code: 0515-561 Client Project: ECTA of Canada Project Start Date: 5/26/15 Sample Type: e-Liquid Analysis Method: ENT301Enthalpy Code Client Code Blank Adjusted Concentrations, ug/mL0515-561-01-1 Acetaldehyde Acetoin# Diacetyl 2,3- ECTA0004-017A Formaldehyde Pentanedione#0515-561-01-2 Notes (ug/mL) (ug/mL) (ug/mL) (ug/mL) (ug/mL) Average 2.88 <0.586 ND 51.5 1.12 J <0.380 ND %DIFF 1.98 J <0.586 ND 45.2 0.974 J <0.380 ND 2.43 <0.586 ND 48.4 1.05 J <0.380 ND 37.1 13.0 14.0 NA NA0515-561-02-1 <0.250 ND <0.586 ND <0.465 ND 1.30 J <0.380 ND ECTA0004-018A <0.250 ND <0.586 ND <0.465 ND 1.66 J <0.380 ND <0.250 ND <0.586 ND <0.465 ND 1.48 J <0.380 ND0515-561-02-2 24.3 NA NA NA NA Average %DIFF0515-561-03-1 <0.250 ND 12.7 11.1 0.449 J <0.380 ND ECTA0004-019A <0.250 ND 12.8 11.2 0.371 J <0.380 ND <0.250 ND 12.7 11.1 0.410 J <0.380 ND0515-561-03-2 NA 0.8 0.5 19.1 NA Average %DIFF # Acetoin is also known as 3-Hydroxy-2-butanone and 2,3-pentanedione is also known as acetyl propionyl.ND: Non Detect or analytical result below the MDL and is less than (<) the reported value. J: Results flagged \"J\" are below the Lower Curve Limit, above the MDL, and are considered estimates.0515-561 ECTA HPLC Carb, Carbs<sV2Page 1 of 1 7/2/20157:55 AM EA# 0515-561 Page 6 of 13

Report for: VapeMate Project Code: 0515-561Client Project: ECTA of Canada Project Start Date: 5/26/15Sample Type: e-Liquid Analysis Methods: ENT058 & 072 Enthalpy Client Code Notes % Water pH Code ECTA0004-017A 0.63 7.920515-561-01 ECTA0004-018A 4.84 5.650515-561-02 ECTA0004-019A 1.23 8.960515-561-030515-561 pH-KFT, sum 7/2/2015Page 1 of 1 7:26 AM EA# 0515-561 Page 7 of 13

Narrative Summary EA# 0515-561 Page 8 of 13

Enthalpy Analytical Narrative Summary Company VapeMate Client Proj ECTA of Canada Analysts KEH, BJB, TMS, JMM Job # 0515-561Parameters ENT184, 301, 058, 072 # Samples 3 e-Liquid samples Custody Summer Mims received samples on 5/26/15 after being relinquished by VapeMate. The samples were received at ambient temperature and in Analysis good condition. Prior to, during, and after analysis, the samples were (Nicotine) kept under lock with access only to authorized personnel by Enthalpy Analytical, Inc. Analysis (DEG) The liquid samples were prepared and analyzed for nicotine and following the analytical procedures in Enthalpy SOP ENT184. Analysis(Carbonyls) The Hewlett Packard Model 6890, Gas Chromatograph “BMO” was equipped with a Flame Ionization Detector and an appropriate column. Analysis(pH & KFT) The samples were prepared and analyzed for diethylene glycol (DEG) following the analytical procedures in Enthalpy SOP ENT184. The Hewlett Packard Model 6890, Gas Chromatograph “BMO” was equipped with a Flame Ionization Detector and an appropriate column. The liquid samples were analyzed for acetaldehyde, acetoin (aka 3- hydroxy-2-butanone), diacetyl, formaldehyde, and 2,3-pentanedione (aka acetyl propionyl) following the procedures in Enthalpy SOP ENT301. The samples were analyzed using the Agilent Model 1100, High Performance Liquid Chromatographs \"Bart\" and “Groucho” equipped with Ultraviolet (UV) Detectors operating at 360 nm and appropriate columns. Samples were measured for pH using an Orion 230A pH meter according the Enthalpy SOP ENT058. Each sample was diluted to a 1% aqueous solution with DI water. Samples were analyzed for water content using the analytical procedures in Method FWN-4604 and Enthalpy SOP ENT072, Determination of % Water by Karl Fischer Titration. The % water results were determined on a Metrohm KFT Titrino Model 795 Titrator. EA# 0515-561 Page 9 of 13

Enthalpy Analytical Narrative Summary (continued) Analysis The 795 KFT uses an internal program and a programmable dosimeter(pH & KFT to dispense titrant. Titrant values were read and printed to an Excelcontinued) spreadsheet.QC Notes All QC samples were within acceptance criteria unless otherwise noted. Formaldehyde was detected in the laboratory blank above the minimum detection limit (MDL) but below the lower curve limit. The results have been blank corrected.Reporting Notes Sample and calibration curve chromatograms are available upon request. The results presented in this report are representative of the samples as provided to the laboratory. Please note that acetoin (aka 3-hydroxy-2-butanone), diacetyl, and 2,3- pentanedione (aka acetyl propionyl) may show false positive results via HPLC/UV in a small percentage of results. These can be confirmed via GC/MS. EA# 0515-561 Page 10 of 13

Sample Receipt RecordEA# 0515-561 Page 11 of 13

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