ftkk_Plant_op_lab

FACULTY OF CHEMISTRYENGINEERING TECHNOLOGYDIRECTORY OF MACHINERIESPLANT OPERATION LABORATORY

PLANT OPERATION LABMACHINE Liquid-Liquid Extraction Unit PRICE -MODEL LL/EV BRAND Electronica VenetaYEAR OF 2002 UNITS 1PURCHASESERIAL NO. 03.01.08794 TAGGING KK-046LOCATION Plant Operation 1, Block A, Academic building1.INTRODUCTIONThis unit includes two separate tanks for the solvent and for the phase having to be refined,that are sent to the extraction column by two metering pumps; the column is providedwith top and bottom phase separators and with two other tanks for collecting the refined andextracted products.

2.SPECIFICATIONS • Framework of AISI 304 stainless steel with castors • Extraction column of borosilicate glass, DN50, consisting of 26 stages, h = 1500 mm, and including stirrer with discs of AISI 316 stainless steel , top and bottom separators of borosilicate glass and variable speed motor (0 to 1000 rpm) with tachogenerator • 4 graduated tanks of borosilicate glass, with capacity of 25 l • Metering double-body pump of AISI 316 stainless steel, with flow rate of 0 to 30 l/h, including pneumatic actuator adjustable with signal of 0.2 to1 bar • Pneumatic control valve of AISI 316 stainless steel, DN 15, Cv = 0.13 • Thermoresistance Pt 100 with sheath of AISI 316 stainless steel • Electronic temperature indicator, 3 manual pneumatic control devices • Piping and valves of AISI 304 and 316 stainless steel • Switchboard IP55, complying with EC conformity mark, including plant synoptic ELCB • Weight: 250kg & Dimension: 2000x900x1800mm3.FUNCTIONExercises on systems of 3 partially mixable components: • acetic acid – toluene – water • acetic acid – isopropyl ether – water • acetic acid – ethyl acetate – water4.COURSES INVOLVE • Diploma in Chemical Engineering Technology • Bachelor in Chemical Engineering Technology5.SUPERVISOR/CO-ORDINATORNo NAME POSITION EMAIL PHONE NO.1 Nurul Aniyyah binti M Tutor [email protected] 0179842588 Sobri

MACHINE Multicyclone System PRICE -MODEL AP01 BRAND SolteqYEAR OF 2002 UNITS 1PURCHASESERIAL NO. 014-0113-AP TAGGING -LOCATION Plant Operation 1, Block A, Academic building1.INTRODUCTIONThis Multi Cyclone System (Model: AP 01) has been manufactured to a high standard withemphasis on ease of use and operational safety. It consists of mainly three cyclones ofdifferent body diameters, a dust feeding system, and an air blower. A flow measurementdevice for the incoming air is also provided. The unit has been designed for studentdemonstration on dust pollution control using cyclone separator.2.SPECIFICATIONS

• Cyclone: 2 units of cyclones made of stainless steelhaving body diameter of 200 mm and 1 unit of cyclone made of borosilicate glass with 100 mm body diameter.Each cyclone has a dust hopper. Appropriate differential pressure tapping points are provided. • Air Blower: 1 unit of 5 hp high pressure blower; maximum capacity @ 3,400 rpm: 280 m3/hr; withstand a static pressure of 80 inches of water; electrical: 415V/ 3- phase/50Hz; comes with inverter for regulating the blower speed. • Air Flowmeter: A venturi type flow meter with DP gauge (max 16 inch of water). • Feeding System: An air pump with dust containers made of clear acrylic. • Differential Pressure: 2 units of differential pressure gauge: 0 to 16 inch of water.3.FUNCTION • To study the effect of inlet velocity upon collection efficiency. • To compare the collection efficiency of powders of different particle sizes. • To study the effect of cyclone body diameter upon collection efficiency. • To compare the overall collection efficiency between single and double cyclone operation. • To verify the theoretical relationship between pressure drop, P and inlet velocity, vi.4.COURSES INVOLVE • Diploma in Chemical Engineering Technology • Bachelor in Chemical Engineering Technology5.SUPERVISOR/CO-ORDINATORBil NAME POSITION EMAIL PHONE NO.1 Nurul Aniyyah binti M Tutor [email protected] 0179842588 Sobri

MACHINE Tray Drier PRICE -MODELYEAR OF PURCHASE BP 722 BRAND SolteqSERIAL NO.LOCATION 2002 UNITS 1 206-0113-BP TAGGING - Plant Operation 1, Block A, Academic building1.INTRODUCTIONThis Tray Drier (Model: BP 772) has been designed for student laboratory trainingprogrammes in unit operations. The unit resembles the most commonly used industrialmethod of drying solids in bulk where hot air stream is passed over fixed trays of wetmaterial. Students will able to vary the operating conditions and collect data to demonstrateboth the theoretical and practical aspects of industrial drying practice.

2.SPECIFICATIONS • Ducting: Horizontal rectangular epoxy coated mild steel duct mounted on a floor standing wheel frame comes with transparent acrylic access door on the wall of the duct. • Electrical Heater: Power rating : 2 kW, Control : Variable transformer, Heating element: Spring coil • Electronic Balance: Capacity : 6,000 g • Fan: Axial fan with speed controller • Instrumentations: fitted with instruments for measuring the air velocity, heater input, and temperature and humidity before and after the heating/drying section3.FUNCTION • Use of psychrometric charts • Energy and mass balances • Demonstration of drying rate regimes • Heat and mass transfer analogies • Drying tests on solid for industrial use • Effect of temperature, air velocity on drying rate4.COURSES INVOLVE • Diploma in Chemical Engineering Technology • Bachelor in Chemical Engineering Technology5.SUPERVISOR/CO-ORDINATORBil NAME POSITION EMAIL PHONE NO.1 Nurul Aniyyah binti M Tutor [email protected] 0179842588 Sobri

MACHINE Rotavapor PRICE -MODEL R 215 BRAND BuchiYEAR OF - UNITS 1PURCHASESERIAL NO. 0700011874 TAGGING -LOCATION Plant Operation 1, Block A, Academic building1.INTRODUCTIONRotavapor R-215 function is for ease of use, safety and the provision of complete solutionsfor evaporation applications. It is design with maximum safety for the user and product andcomplete solution with vacuum controller, vacuum pump and recirculating chiller

2.SPECIFICATIONS • Voltage: 100-240 VAC • Frequecy: 50/60 Hz • Power 60 W • Weight : 16-18kg • Rotation Speed: 20-280rpm • Flask size: 50-4000ml • Maximum flask capacity: 3kg • Display: Rotation speed and vapour temperature3.FUNCTION • Evaporation of solvents4.COURSES INVOLVE • Diploma in Chemical Engineering Technology • Bachelor in Chemical Engineering Technology5.SUPERVISOR/CO-ORDINATORBil NAME POSITION EMAIL PHONE NO.1 Nurul Aniyyah binti M Tutor [email protected] 0179842588 Sobri

MACHINE Solid Liquid Extraction PRICE -MODEL D55122 BRAND QVFYEAR OF - UNITS 1PURCHASESERIAL NO. 5022682/463 D TAGGING -LOCATION Operation Unit 1 Lab, Block A, Academic building1.INTRODUCTIONThe plant is fitted with an external steam or electrically heated thermosyphon reboiler. Presolvent vapor generated in the boiler rises through the jacketed column and is condensed ina vertical water-cooled condenser. Liquid solvent passes through a solvent cooler whichcontrols the solvent temperature-a flow rate indicator and into the extraction chamber. Thesolvent is directed either upward through the soled bed or downward through a sparge ring.The extract solution passes into the reboiler when pure solvent is regenerated. Samples ofextract solution and reboiler contents can be taken and their compositions determined bydensity measurement.

2. SPECIFICICATIONS 6 litre ball vessel made of borosilicate glassEvaporator B1 with bottom outlet 1700 W safety heating mantle withHeating cover W1 temperature controller Column section DN 50 made of borosilicateColumn K glass height: 1000 mm packing: glassRASCHIG rings Vertical coil heat exchanger made of heatCondenser W2 transfer area: 0.3 m2 Vertical coil heat exchanger made ofProduct cooler W3 borosilicate glass heat transfer area: 0,1 m2 Extraction vessel B3: vessel with quickReceiver B2 closure unit insert unit for approximately 3 to 4 liter raw material made of borosilicate glassPre-heater W4 250W with temperature control (only for heat extraction)Frame Tubular frame supportOperating conditions Pressure: Normal Pressure, vacuum temperature: max. 150 celcius.REQUIREMENTSElectrical supply 240VAC/1-Phase/50HZWater supply Cold water at 20LPM@3m headOVERALL DIMENSIONSHeight 3.00 mWidth 1.00 mDepth 0.603.FUNCTIONEXPERIMENTAL CAPABILITIES • Straight- through extraction • Over flow extraction • SOXHLET extractionAfter completion of the extraction process, the extract can be further purified by distilling offthe solvent.

4.COURSES INVOLVE • Diploma in chemical engineering technology • Bachelor in chemical engineering technology5.SUPERVISOR / CO-ORDINATORBil NAME POSITION EMAIL PHONE NO. [email protected] 01798425881 Nurul Aniyyah Tutor binti M Sobri

MACHINE Distillation Bubble Cap PRICE - ColumnMODEL BRAND SOLTEQ-QVFYEAR BP04 UNITS 1PURCHASESERIAL NO. OF -LOCATION - TAGGING - Operation Unit 1 Lab, Block A, Academic building1.INTRODUCTIONA complete teaching system with comprehensive experiments, data analysis, tutor andstudent’s manual, all instruments and controllers. • Vacuum or atmospheric operation • Bath or steady state distillation • Custom designed for technician/ under-graduate teaching • Complete visual monitoring of the process • Easily operated and used • Suitable for project or research work

2.SPECIFICATIONSA QVF distillation teaching system module comprising an 80 mm, 8 tray bubble cap column,20 litre thermosyphon boiler, vapour condenser, infinitely variable reflux control, distillatecooler and receiver, all manufactured in borosilicate glass. Flameproof, designed as a batchrectifier or continuous enricher with atmospheric or vacuum operation. Supplied with allvalves, controllers, instrumentation, services lines and supporting structure. Complete with atutor’s manual, 25 student manuals, 25 experiment booklets for each experiment, aninstallation and maintenance manual and tool kit.3.FUNCTIONEXPERIMENTAL CAPABILITIES • Mass and heat balances • Vapour/ liquid equilibria • Determination of vapour and liquid flowrates • Determination of heat flows within the plant • The effect of varying the reflux ratio • Determination of column efficiency using McCabe Thiele and Ponchon Savarit constructions • Batch distillation with constant reflux control • Batch distillation with constant product control • Distillation under vacuumA methanol/ water mixture is used in all experiments. Other binary mixtures can also beinvestigated. The experiments are also designed to provide training in chemical plant controland opration.4.COURSES INVOLVE • Diploma in chemical engineering technology • Bachelor in chemical engineering technology5.SUPERVISOR / CO-ORDINATORBil NAME POSITION EMAIL PHONE NO. [email protected] 01798425881 Nurul Aniyyah Tutor binti M Sobri

MACHINE Climbing Film Evaporation PRICE -MODEL BP04 BRAND SOLTEQ-QVFYEAR OF - UNITS 1PURCHASESERIAL NO. - TAGGING -LOCATION Operation Unit 1 Lab, Block A, Academic building1.INTRODUCTIONA complete teaching system with comprehensive experiments, data analysis, tutor andstudents’s manuals, all instruments and controllers. • Vacuum or atmospheric operation • Bath or continuous operation • Optional forced circulation • Custom designed for technician / under- graduate teaching • Complete visual monitoring of the process • Easily operated and used • Suitable for project or research work.

2.SPECIFICATIONA QVF evaporation teaching system module comprising a 3000 mm * 25 mm diameter longtube evaporator, cyclone separator, vapour condenser, product and condensate receiver, allmanufactured in borosilicate glass. Flameproof, designed to operate as either a climbing filmor natural circulation evaporator with atmospheric or vacuum operation. Supplied with allvalves, controllers, instrumentation, service lines and supporting structure. Complete with atutor’s manual, 25 student manuals, 25 experiment booklets for each experiment, aninstallation and maintenance manual and tool kit.3.FUNCTIONEXPERIMENTAL CAPABILITIES • Mass and heat balances • Determination of evaporative heat transfer coefficients • Influence of vacuum levels on evaporation rates • Influence of system pressure on evaporation rates • Influence of flow rate on forced circulation heat transfer coefficients. • Comparison pf climbing film, natural and forced circulation evaporation.Water is used in all experiment; climbing film evaporation is particularly suited to theconcentration of heat sensitive material such as milk, fruit juices, blood plasma, etc and fordesalination studieds.4.COURSES INVOLVE • Diploma In Chemical Engineering Technology • Bachelor In Chemical Engineering Technology5.SUPERVISOR / CO-ORDINATORBil NAME POSITION EMAIL PHONE NO. [email protected] 01798425881 Nurul Aniyyah Tutor binti M Sobri

MACHINE Laboratory Test Sieve PRICE -MODEL - BRAND ENDECOTTSYEAR OF - UNITS 1PURCHASESERIAL NO. OCT-6212-10 TAGGING -LOCATION Operation Unit 1 Lab, Block A, Academic building1.INTRODUCTIONA test sieve consists of a woven wire screen, with square apertures, rigidly mounted in ashallow cylindrical metal frame. For coarse sieving a perforated plate screen with square orround holes may be used in place of wire mesh. Square hole perforated plate sieves rangedown to 4 mm and round hole sieves down to 1 mm aperture. The sizes of solid particlesfrom 125 mm down to 20 µm can be measured rapidly and efficiently by means of standardtest sieves. Special sieves with apertures smaller than 20 µm are available, but it should beappreciated that finer a screen is, the more easily will certain types of particulate solids tendto block or blind the apertures. Nevertheless, 'micro' sieving can be carried out down to 5 µmusing special techniques. Particle size, as measured by test sieving, may be specified simplyby quoting two sieve sizes, one through which particles have passed, and the other on whichthey are retained.

2.SPECIFICATION • Suitable for dry sieving: yes • Suitable for wet sieving: yes • Electrical supply: different voltages available • Interval operation: yes (one mode) • Net weight: 43 kg3.FUNCTIONEXPERIMENTAL CAPABILITIES • Used for measurement of particle size • Used for measuring the size spread, i.e., the particle size distribution. • When the size distribution of a sample has been determined by test sieving, the material becomes separated into several fractions.4.COURSES INVOLVE • Diploma In Chemical Engineering Technology • Bachelor In Chemical Engineering Technology5.SUPERVISOR / CO-ORDINATORBil NAME POSITION EMAIL PHONE NO. 01798425881 Nurul Aniyyah Tutor [email protected] binti M Sobri

MACHINE Gas Absorption Unit PRICE -MODEL ET-3221-GAC BRAND BENUATECHYEAR OF - UNITS 1PURCHASESERIAL NO. 5016500 TAGGING -LOCATION Plant Operation 1, Block A, Academic building1. INTRODUCTIONGas absorption is a process in which the soluble parts of a gas mixture are transferred to ordissolved in a liquid. The reverse process, called desorption or stripping, is used to transfervolatile parts from a liquid mixture to a gas.

2. SPECIFICATIONS • Air Receiver • Separation of CO2/air mixture by absorption in counterflow with water • Adjustment of mixing ratio using valve • Water temperature control with heater and refrigerant system • Production of gas mixture using CO2 from compressed gas cylinder and ambient air3. FUNCTION • To remove one or more gaseous components from a gas flow using a solvent4. COURSES INVOLVE • Diploma in Chemical Engineering Technology • Bachelor in Chemical Engineering Technology5. SUPERVISOR/CO-ORDINATORBil NAME POSITION EMAIL PHONE NO.1 Nurul Aniyyah binti M Tutor [email protected] 0179842588 Sobri

MACHINE Cooling Tower PRICE -MODEL - BRAND 1YEAR OF UNITSPURCHASESERIAL NO. 3036 TAGGING -LOCATION Plant Operation 1, Block A, Academic building1. INTRODUCTIONThe cooling tower was originally developed as a water conservation device, designed toreduce dependence on ‘once through’ cooling systems and successfully replaced many suchsystems. The development of the cooling tower also expanded the ability of designers toprovide efficient cooling in areas without large water supplies. Cooling towers are nowapplied widely across a range of industries; however they are not always applied efficientlyor optimally.

2. SPECIFICATIONS • Heater • Fan • Pump • Cooling Column3. FUNCTION • Cooling towers are heat exchangers that use water and air to transfer heat from air- conditioning systems to the outdoor environment.4. COURSES INVOLVE • Diploma in Chemical Engineering Technology • Bachelor in Chemical Engineering Technology5. SUPERVISOR/CO-ORDINATORBil NAME POSITION EMAIL PHONE NO.1 Nurul Aniyyah binti M Tutor [email protected] 0179842588 Sobri

MACHINE Electric Boiler PRICE -MODEL EP 72 BRAND FULTONYEAR OF - UNITS 1PURCHASESERIAL NO. EB 2963 TAGGING -LOCATION Plant Operation 1, Block A, Academic building1. INTRODUCTIONElectric boilers are a method of heating hot water for your heating system using onlyelectricity. A typical boiler uses gas to heat the water, whilst an electric boiler can be used inoff-grid areas or where a gas supply is either not wanted or not possible.

2. SPECIFICATIONS • EP72 models have an integrated feed water tank and feed water pump, all in one compact unit. • Output: 95 kg/h (F&A 100°C) • Operating Pressure: 11.2 barg • Safety Valve Pressure: 7.93 bar • Electrical Requirement: FLC 400 V 3 ph 50 Hz • Max Continous Rating: 72 kW3. FUNCTION • Main function to convert water into steam. • To generate steam with using a heating element.4. COURSES INVOLVE • Diploma in Chemical Engineering Technology • Bachelor in Chemical Engineering Technology5. SUPERVISOR/CO-ORDINATORBil NAME POSITION EMAIL PHONE NO.1 Nurul Aniyyah binti M Tutor [email protected] 0179842588 Sobri