FTKK Chem Tech Lab

FACULTY OF CHEMISTRY ENGINEERING TECHNOLOGYDIRECTORY OF MACHINERIESCHEMICAL TECHNOLOGY LAB

CHEMICAL TECHNOLOGY LABMACHINE High Performance Liquid PRICE - ChromatographyMODEL 1100 series BRAND AgilentYEAR OF 2005 UNITS 1PURCHASESERIAL NO. DE23930456 TAGGING kk-050LOCATION Unit operation 2 lab, Block B, Academic building1. INTRODUCTION The HP/Agilent 1100 series is the current model and arguably the best design in the industry because of the optimized design of the quaternary pump ensuring virtually pulse-free and stable solvent flow, with dual floating pistons in series, precisely serve-controlled. This design with variable stroke volume allows pulse-free solvent delivery and efficient mixing. An inlet-valve electronically activated and synchronized to piston stroke – eliminates vapor formation with volatile solvent and is maintenance free. With high-speed proportioned valve and preconfigured vacuum degasser, it is convenient for low – pressure mixing of up to four solvents and highest flexibility in solvent choices.

2. SPECIFICATIONSPhysical Specifications For your PC specifications refer to its documentation.Type Specification Comments Weight 11.0 kg (25.0 lbs) 11.0 kg (25.0 lbs) 10.2 kg (22.5 lbs)17.0 kg (38.0 lbs) G1310A ISO Pump G1314A VWD G1316A TCC G1362ARID Dimensions (width × depth × height) 345 × 435 × 140 mm (13.5 × 17 × 5.5 inches) 345× 435 × 180 mm (13.5 × 17 × 7.0 inches) 410 × 435 × 140 mm (16.1 × 17 × 5.5 inches)G1310A, G1314A, G1321A G1362A G1316ALine Voltage 100 – 120 or 220 – 240 VAC, ± 10 % Wide-ranging capability Line frequency50 or 60 Hz, ± 5 % Power consumption 320 VA maximum 160 VA maximum G1362AAmbient operating temperature 0 – 55 °C (32 – 131 °F)Ambient non-operating temperature -40 – 70 °C (-4 – 158 °F) Humidity3. FUNCTIONHPLC stands for HPLC. It is a liquid chromatography which involves the separation of thecompounds on the basis of their polarity. It is used to analyze, identify, purify & quantify thecompound4. COURSES INVOLVE• Diploma in chemical technology• Bachelor in chemical technology5. SUPERVISOR/CO-ORDINATORBil NAME POSITION EMAIL PHONE NO.1 Abdul Hadi B Abdullah Instructor [email protected] 0183894498

MACHINE Gas Chromatography PRICE -MODEL 6890N (G1540N) BRAND AgilentYEAR OF 2006 UNITS 1PURCHASESERIAL NO. US10302068 TAGGING kk-051LOCATION Unit operation 2 lab, Block B, Academic building1. INTRODUCTIONChromatography is a dynamic separation process based on differences in the rates of migrationof different compounds through a column containing an immobilised phase. Migration is inducedby a continuous flow of the mobile phase through the column.In general chromatography is based on the selective distribution of the different componentsbetween two phases. One of the phases, the stationary phase, is held immobilised inside thecolumn while the other phase, the mobile phase travels through the column, flowing through thestationary phase. Compounds that exhibit a higher affinity for the stationary phase will travelmore slowly than compounds exhibiting a lower affinity. The different sample components travelat different speed through the column and are eluted from the column at different times. Thecolumn should be sufficiently long to obtain the desired degree of separation.

2. SPECIFICATIONS• Height: 50 cm (19.7 in)• Width: 58 cm (22.8 in) with EPC inlet and detectors; 68 cm (26.8 in) with manual inlets ordetectors or with optional gauges• Depth: 54 cm (21.6 in) Average weight: 49 kg (108 lb)• Clock time programming• Run deviation log (notes any changes to setpoints or expected values during a run, savedwith run file in ChemStations) - Promote control of eight external events (valves, on/off, orlowlevel contact)• Four internal 24-volt connections (up to 150 mA)• Two external 24-volt connections (up to 75 mA)• Two on/off contact closures (48 V, 250 mA max)3. FUNCTION • Determination of volatile compound (gases and liquid) • Determination of partition coefficient and absorption isotherms • Isolating pure component from complex mixtures4. COURSES INVOLVE • Diploma in chemical technology • Bachelor in chemical technology5. SUPERVISOR/CO-ORDINATORBil NAME POSITION EMAIL PHONE NO.1 Abdul Hadi B Abdullah Instructor [email protected] 0183894498

MACHINE Fourier Transform Infra Red PRICE -MODEL Spectrum RX1 BRAND Perkin ElmerYEAR OF - UNITS 1PURCHASESERIAL NO. 67993 TAGGING kk-043LOCATION Unit operation 2 lab, Block B, Academic building1.INTRODUCTIONAn FT-IR Spectrometer is an instrument which acquires broadband NIR to FIR spectra. Unlike adispersive instrument, i.e. grating monochromator or spectrograph, FT-IR SpectrometerSelection Guide< collect all wavelengths simultaneously. This feature is called the Multiplex orFelgett Advantage.FT-IR Spectrometers are often simply called FTIRs. But for the purists, an FT-IR (FourierTransform InfraRed) is a method of obtaining infrared spectra by first collecting an interferogramof a sample signal using an interferometer, and then performing a Fourier Transform (FT) on theinterferogram to obtain the spectrum. An FT-IR Spectrometer collects and digitizes theinterferogram, performs the FT function, and displays the spectrum.

2. SPECIFICATIONS FR DTGS DETECTOR LiTaO3Wavelength range 7,800 – 350 cm-1 with Kbr beamsplitter 7,800 – 350 cm-1 with KBrResolution beamsplitterWavelength accuracy 0.5 cm-1 to 64 cm-1Signal to noise ratio for KBr 0.1 cm-1 at 1,600 cm-1 7,800 – 225 cm-1 with CsIoptic beamsplitter 0.5 cm-1 to 64 cm-1Available OPD velocities 0.1 cm-1 at 1,600 cm-1 30,000/1 rms, 6,000/1 p-p for 7,500/1 rms, 1,500/1 p-p for a a 5 second measurement and 5 second measurement and 100,000/1 rms, 20,000/1 p-p 26,000/1 rms, 5,000/1 p-p for for a 1 minute measurement a 1 minute measuremen 0.1, 0.2, 0.5, 1 and 2 cms-1 0.1, 0.2, 0.5, 1 and 2 cms-13. FUNCTIONFourier Transform Infra Red (FTIR) could be determined of polymer and rubber characteristic.4. COURSES INVOLVE • Diploma in chemical technology • Bachelor in chemical technology5. SUPERVISOR/CO-ORDINATORBil NAME POSITION EMAIL PHONE NO.1 Abdul Hadi B Abdullah Instructor [email protected] 0183894498

MACHINE Atomic Absorption PRICE - SpectrometerMODEL Aanalyst400 BRAND Perkin ElmerYEAR OF - UNITS 1PURCHASESERIAL NO. 201S2121116 TAGGING kk-046LOCATION Unit operation 2 lab, Block B, Academic building1.INTRODUCTIONAtomic-absorption (AA) spectroscopy uses the absorption of light to measure the concentrationof gas-phase atoms. Since samples are usually liquids or solids, the analyte atoms or ions mustbe vaporized in a flame or graphite furnace. The atoms absorb ultraviolet or visible light andmake transitions to higher electronic energy levels.The analyte concentration is determined from the amount of absorption. Applying the Beer-Lambert law directly in AA spectroscopy is difficult due to variations in the atomization efficiencyfrom the sample matrix, and nonuniformity of concentration and path length of analyte atoms (ingraphite furnace AA). Concentration measurements are usually determined from a workingcurve after calibrating the instrument with standards of known concentration.

2. SPECIFICATIONSDimensions 70 x 65 (0.46 m2 ) x 65 cm (W x D x H)Weight 49 kgPower 100-230 V (±10%), 50/60 Hz (±1%), 300 VA (maximum)Technical Classified as a laboratory instrument. Complies with the applicable European Union directives and standards for safety and electromagnetic compatibility for CE Marking, the safety requirements for Canada and the United States for CSA/NRTL certification and the FCC requirements for radio-frequency emissions. The instrument was developed and produced in compliance with ISO 9001.Environmental Dust-free, free of vibrations, ambient temperatures: +15 ˚C to +35 ˚C with a change rate of a maximum 3 ˚C per hour. Relative humidity: 20% to 80% non-condensing.3. FUNCTION • Detect heavy metal • Waste water analysis4. COURSES INVOLVE • Diploma in chemical technology • Bachelor in chemical technology5. SUPERVISOR/CO-ORDINATORBil NAME POSITION EMAIL PHONE NO.1 Amri B Hj Mohamed Instructor [email protected] 0183894498

MACHINE Differential Scanning PRICE - Calorimetry (DSC)MODEL TGA851 BRAND Mettler ToledoYEAR OF PURCHASE 2007 UNITS 1SERIAL NO. TATIUC 21/7/01LOCATION SF/1100 TAGGING Unit operation 2 lab, Block B, Academic building1.INTRODUCTIONDifferential scanning calorimetry, or DSC, is a thermoanalytical technique in which thedifference in the amount of heat required to increase the temperature of a sample and referenceis measured as a function of temperature.

2. SPECIFICATIONSTEPERATURETemperature range Air cooling : RT – 700oc Cryostat cooling : -50 oc - 700 oc Intra cooler :-650 oc- 700 oc Liquid nitrogen cooling:-150 oc- 700 ocAccuracy : ± 0.2 ocReproducibility : ± 0.1 ocHeating rate RT- 500 oc:- RT- 700 oc: 5MINProgrammable heating rates : 0- 100 K/min (at 700 oc), smallest increment 0.01 K/minCooling ratea) Air cooling from max temperature to 100 oc : 9 minb) Cryostat cooling from 100 to 0 oc : 5 minc) Intracooler from 100 to 0 oc : 4 mind) Liquid nitrogen cooling from 100 to -100 oc : 15 min2. FUNCTION• To study thermal analysis of a material and differential scanning calorimeter• To observe more subtle phase changes, such as glass transitions• To measure a number of characteristic properties of a sample4. COURSES INVOLVE• Diploma in chemical technology• Bachelor in chemical technology5. SUPERVISOR/CO-ORDINATORBil NAME POSITION EMAIL PHONE NO.1 Mashelmie B Sidik Instructor [email protected] 0139145861

MACHINE Thermogravimetric Analysis PRICE - (TGA)MODEL TGA851 BRAND Mettler ToledoYEAR OF PURCHASE 2007 UNITS 1SERIAL NO. TATIUC 21/7/01LOCATION SF/1100 TAGGING Unit operation 2 lab, Block B, Academic building1.INTRODUCTIONThermogravimetric analysis (TGA) is a type of thermal analysis for polymer. Other thermalanalyses include differential scanning calorimetry (DSC) and differential thermal analysis.Thermal analysis is important in order to study the variety of responses of the material toenthalpy changes, temperature, heating, degradation or other chemical changes.

2. SPECIFICATIONSTEPERATURERrange :RT-1100 ocAccuracy : ± 0.25 ocReproducibility : ± 0.15 ocCooling timeNot regulated from 1000 oc to 100 oc : 22 minBALANCEBalance type : MT5Measuring range : 38KgDIMENSIONSWidth x depth x height :52x278x646 mmWeight : 38Kg3. FUNCTION • To determine the percentage component in a compound • The percentage of weight loss • The different composition in the blend • To study thermal analysis of a material4. COURSES INVOLVE • Diploma in chemical technology • Bachelor in chemical technology5. SUPERVISOR/CO-ORDINATORBil NAME POSITION EMAIL PHONE NO.1 Mashelmie B Sidik Instructor [email protected] 0139145861

MACHINE Auto Lab PRICE -MODEL Metrohm BRAND Mettler ToledoYEAR OF PURCHASE UNITS 1SERIAL NO. PGSTAT128N TAGGINGLOCATION Unit operation 2 lab, Block B, Academic building1.INTRODUCTIONThe entry level member of the modular Autolab instruments family, the PGSTAT128N is a lowcurrent, low noise and fast potentiostat/galvanostat capable of measuring maximum 800 mA,with a compliance voltage of 12 V. The PGSTAT128N is a high performance low cost option forelectrochemical measurements in small cells.Designed for a wide range of electrochemical applications, from corrosion measurements to thecharacterization of energy storage devices, this budget instrument is the ideal choice forelectrochemical applications where performance is important. You can customize and enhancethe capabilities of the PGSTAT128N by adding one or more of the many availableoptional modules or accessories.

2. SPECIFICATIONS 2, 3 and 4 +/- 10 VElectrode connectionsPotential range +/- 12 VCompliance voltage +/- 800 mA (10 A with BOOSTER10A)Maximum current 1 A to 10 nA (100 pA with ECD module)Current ranges +/- 0.2 %Potential accuracy 0.3 µVPotential resolutionCurrent accuracy +/- 0.2 %Current resolution 0.0003 % (of current range)Input impedancePotentiostat bandwidth > 1 TOhmComputer interface 500 kHz USB3.FUNCTION• DC and AC electrochemical measurements on large area electrodes• Determination of charge/discharge characteristics of super-capacitors• Electrochemical impedance at high current densities• Measurements of the i-V and power characteristics of energy storage devices4. COURSES INVOLVE • Bachelor in chemical technology ( final year project )5. SUPERVISOR/CO-ORDINATORBil NAME POSITION EMAIL PHONE NO.1 Abdul Hadi B Abdullah Instructor [email protected] 0199531241

MACHINE UV Spectrophotometer PRICE -MODEL UV1800 BRAND ShidmazuYEAR OF PURCHASE UNITS 1SERIAL NO. TAGGINGLOCATION Unit operation 2 lab, Block B, Academic building1.INTRODUCTIONThe entry level member of the modular Autolab instruments family, the PGSTAT128N is a lowcurrent, low noise and fast potentiostat/galvanostat capable of measuring maximum 800 mA,with a compliance voltage of 12 V. The PGSTAT128N is a high performance low cost option forelectrochemical measurements in small cells.Designed for a wide range of electrochemical applications, from corrosion measurements to thecharacterization of energy storage devices, this budget instrument is the ideal choice forelectrochemical applications where performance is important. You can customize and enhancethe capabilities of the PGSTAT128N by adding one or more of the many availableoptional modules or accessories.

2. SPECIFICATIONS 190 to 1100nm 1nm (190 to 1100nm)Wavelength range 0.1-nm incrementsSpectral bandwidth 0.1-nm increments (1-nm incrementsWavelength display when setting scanning range )Wavelength setting ±0.1nm at 656.1nm D2 ±0.3nm (190 to 1100nm)Wavelength accuracy ±0.1nm Double BeamWavelength repeatabilityPhotometric system 15kg USB memory (option) Saved as textWeight and UVPC fileMemory3.FUNCTION • UV/Vis spectroscopy is routinely used in analytical chemistry for the quantitative. • determination of different analytes, such as transition metal ions, highly conjugated organic compounds, and biological macromolecules. • Solvent polarity and pH can affect the absorption spectrum of an organic compound.4. COURSES INVOLVE • Bachelor in chemical technology ( final year project ) • Dip of chemical technology5. SUPERVISOR/CO-ORDINATORBil NAME POSITION EMAIL PHONE NO.1 Abdul Hadi B Abdullah Instructor [email protected] 0199531241